2A6R
Crystal structure of YoeB under PEG condition
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-05-28 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.00000 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 163.898, 43.138, 89.367 |
Unit cell angles | 90.00, 118.49, 90.00 |
Refinement procedure
Resolution | 14.980 - 2.050 |
R-factor | 0.198 |
Rwork | 0.196 |
R-free | 0.22900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | extracted from YoeB structure from 2A6Q |
RMSD bond length | 0.005 |
RMSD bond angle | 1.200 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.720 | 2.120 |
High resolution limit [Å] | 2.050 | 2.050 |
Number of reflections | 34757 | |
<I/σ(I)> | 19.99 | |
Completeness [%] | 99.6 | 95.1 |
Redundancy | 3.6 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293.2 | Tris-HCl, MgCl, PEG8000, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 293.2K |