2A2F
Crystal Structure of Sec15 C-terminal domain
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 298 |
Detector technology | CCD |
Collection date | 2003-12-01 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.97958,0.97949,0.96308 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 80.500, 93.900, 123.500 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 500.000 - 2.500 |
Rwork | 0.243 |
R-free | 0.27600 |
Structure solution method | MAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.260 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 500.000 | 2.590 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 15141 | |
Completeness [%] | 91.5 | 80.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 298 | sodium Citrate, ammonium phosphate, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 298 | sodium Citrate, ammonium phosphate, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 298 | sodium Citrate, ammonium phosphate, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K |