2ZL1
MP1-p14 Scaffolding complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X29A |
Synchrotron site | NSLS |
Beamline | X29A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-02-18 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0809 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 44.290, 62.440, 74.980 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.000 - 2.000 |
R-factor | 0.20515 |
Rwork | 0.203 |
R-free | 0.25602 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.402 |
Data scaling software | d*TREK (9.5L) |
Refinement software | REFMAC (5.4.0069) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 48.000 | 32.540 | 2.070 |
High resolution limit [Å] | 2.000 | 4.310 | 2.000 |
Rmerge | 0.056 | 0.032 | 0.342 |
Total number of observations | 8153 | 8040 | |
Number of reflections | 14618 | ||
<I/σ(I)> | 12.7 | 30.1 | 3.9 |
Completeness [%] | 100.0 | 100 | 100 |
Redundancy | 5.52 | 5.12 | 5.57 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 295 | 11%(w/v) PEG 3350, 0.1M HEPES, pH 7.5, vapor diffusion, hanging drop, temperature 295K |