2YXV
The deletion mutant of Multicopper Oxidase CueO
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2007-03-07 |
Detector | RIGAKU |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 |
Unit cell lengths | 49.982, 50.947, 86.050 |
Unit cell angles | 83.20, 90.83, 66.66 |
Refinement procedure
Resolution | 24.400 - 1.810 |
R-factor | 0.1724 |
Rwork | 0.171 |
R-free | 0.20778 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.384 |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 25.940 |
High resolution limit [Å] | 1.810 |
Number of reflections | 62169 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 16% PEG 3350, 0.16M Potassium Nitrate, 20% Glycerol, VAPOR DIFFUSION, temperature 293K |