2YB7
CBM62 in complex with 6-alpha-D-Galactosyl-mannotriose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU IMAGE PLATE |
Spacegroup name | F 2 3 |
Unit cell lengths | 191.352, 191.352, 191.352 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 110.430 - 1.700 |
R-factor | 0.16607 |
Rwork | 0.165 |
R-free | 0.18565 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2Y9S |
RMSD bond length | 0.032 |
RMSD bond angle | 2.578 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 110.400 | 1.790 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.150 | 0.900 |
Number of reflections | 60268 | |
<I/σ(I)> | 14 | 1.8 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.4 | 7.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.4 | 0.5 M AMMONIUM SULPHATE IN 0.1 M NA/HEPES, PH 7.4, CONTAINING 30 % 2-METHYL-2,4-PENTANEDIOL. |