2Y5F
FACTOR XA - CATION INHIBITOR COMPLEX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-04-23 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 48.937, 74.300, 77.201 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.290 |
R-factor | 0.13982 |
Rwork | 0.138 |
R-free | 0.17470 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2jkh |
RMSD bond length | 0.013 |
RMSD bond angle | 1.748 |
Data reduction software | XDS |
Data scaling software | SADABS |
Phasing software | CCP4 |
Refinement software | REFMAC (5.6.0093) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.310 |
High resolution limit [Å] | 1.290 | 1.290 |
Rmerge | 0.060 | 0.740 |
Number of reflections | 71523 | |
<I/σ(I)> | 14.56 | 1.45 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 7.2 | 7.12 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |