2XZ3
BLV TM hairpin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-04-11 |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | H 3 |
Unit cell lengths | 107.595, 107.595, 119.170 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 25.000 - 1.950 |
R-factor | 0.19445 |
Rwork | 0.192 |
R-free | 0.23693 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1mg1 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.383 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.5.0088) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.000 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.040 | 0.570 |
Number of reflections | 37151 | |
<I/σ(I)> | 23.9 | 2.1 |
Completeness [%] | 99.0 | 90 |
Redundancy | 3.5 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.6 | 24.5%(V/V) ISOPROPANOL, 13.5%(V/V) PEG 4000, 0.1M SODIUM CITRATE, PH 5.6 |