2XYP

Caspase-3:CAS26049945

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	ENRAF-NONIUS FR591
Temperature [K]	100
Spacegroup name	I 2 2 2
Unit cell lengths	69.569, 83.782, 95.805
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 1.860
R-factor	0.1667
Rwork	0.167
R-free	0.20440
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.005
RMSD bond angle	1.246
Refinement software	CNS

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	1.860
Rmerge	0.040
Number of reflections	23519
<I/σ(I)>	27.8
Completeness [%]	99.3
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1