Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | MAX II BEAMLINE I911-5 |
| Synchrotron site | MAX II |
| Beamline | I911-5 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-01-24 |
| Detector | MARRESEARCH SX-165 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 42.060, 42.060, 202.910 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 24.784 - 1.820 |
| R-factor | 0.2051 |
| Rwork | 0.203 |
| R-free | 0.23950 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.052 |
| Data reduction software | MOSFLM |
| Data scaling software | XIA |
| Phasing software | PHASER |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 28.990 | 1.870 |
| High resolution limit [Å] | 1.820 | 1.820 |
| Rmerge | 0.040 | 0.500 |
| Number of reflections | 19558 | |
| <I/σ(I)> | 23.1 | 3 |
| Completeness [%] | 99.5 | 95.9 |
| Redundancy | 4.6 | 4.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8.5 | 30 % PEG-4000, 0.2 M SODIUM ACETATE TRIHYDRATE, 0.1 M TRIS HYDROCHLORIDE PH 8.5. |
