2XVN
A. fumigatus chitinase A1 phenyl-methylguanylurea complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF |
| Synchrotron site | ESRF |
| Beamline | ID14-2 |
| Temperature [K] | 287 |
| Spacegroup name | P 32 |
| Unit cell lengths | 99.985, 99.985, 111.301 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 12.000 - 2.350 |
| R-factor | 0.25936 |
| Rwork | 0.259 |
| R-free | 0.29861 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.023 |
| RMSD bond angle | 2.019 |
| Refinement software | REFMAC (5.5.0088) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 2.350 |
| Rmerge | 0.110 |
| Number of reflections | 51912 |
| Completeness [%] | 98.5 |
| Redundancy | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
