2XUS
Crystal Structure of the BRMS1 N-terminal region
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-11-20 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | H 3 2 |
Unit cell lengths | 60.399, 60.399, 133.485 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.701 - 1.912 |
R-factor | 0.204 |
Rwork | 0.200 |
R-free | 0.27540 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ccf |
RMSD bond length | 0.018 |
RMSD bond angle | 1.478 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.700 | 2.020 |
High resolution limit [Å] | 1.910 | 1.910 |
Rmerge | 0.040 | 0.280 |
Number of reflections | 7517 | |
<I/σ(I)> | 79.3 | 14.5 |
Completeness [%] | 99.7 | 100 |
Redundancy | 40.4 | 30.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.25 | 0.1 M SODIUM CITRATE PH 5.25, 1.5 M AMMONIUM SULPHATE |