Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 287 |
| Detector technology | AREA DETECTOR |
| Detector | MULTIWIRE |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 59.600, 102.400, 56.100 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 24.634 - 2.052 |
| R-factor | 0.1448 |
| Rwork | 0.142 |
| R-free | 0.19170 |
| Structure solution method | MIR |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.010 |
| RMSD bond angle | 0.948 |
| Phasing software | MLPHARE |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 24.600 |
| High resolution limit [Å] | 2.050 |
| Number of reflections | 19617 |
| Completeness [%] | 88.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | 12% PEG8000, 50 MM MOPS PH7.0 |
