2XQY
CRYSTAL STRUCTURE OF PSEUDORABIES CORE FRAGMENT OF GLYCOPROTEIN H IN COMPLEX WITH FAB D6.3
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2010-03-28 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 82.310, 100.630, 161.830 |
| Unit cell angles | 90.00, 94.02, 90.00 |
Refinement procedure
| Resolution | 58.120 - 2.050 |
| R-factor | 0.1887 |
| Rwork | 0.188 |
| R-free | 0.20460 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1bbd |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.020 |
| Data reduction software | autoPROC |
| Data scaling software | autoPROC |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 58.130 | 2.160 |
| High resolution limit [Å] | 2.050 | 2.050 |
| Rmerge | 0.040 | 0.490 |
| Number of reflections | 151575 | |
| <I/σ(I)> | 22.3 | 1.3 |
| Completeness [%] | 92.1 | 55.3 |
| Redundancy | 6.1 | 2.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8 | 0.1M IMIDAZOLE PH 8, 0.7M SODIUM FORMATE, 10.5% PEG 4,000 |
