2XMO
The crystal structure of Lmo2642
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 4A |
| Synchrotron site | PAL/PLS |
| Beamline | 4A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 62.963, 103.267, 73.765 |
| Unit cell angles | 90.00, 102.80, 90.00 |
Refinement procedure
| Resolution | 30.000 - 1.700 |
| R-factor | 0.2118 |
| Rwork | 0.212 |
| R-free | 0.24250 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.247 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | CNS (1.2) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.730 |
| High resolution limit [Å] | 1.700 | 1.700 |
| Rmerge | 0.090 | 0.390 |
| Number of reflections | 93909 | |
| <I/σ(I)> | 13.8 | 1.5 |
| Completeness [%] | 93.1 | 63.2 |
| Redundancy | 5.4 | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.2 | 20% PEG3350, 0.4M SODIUM FORMATE, pH 7.2 |
