2XJY
Crystal structure of the LMO2:LDB1-LID complex, P21 crystal form
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-2 |
| Synchrotron site | ESRF |
| Beamline | ID23-2 |
| Temperature [K] | 77 |
| Detector technology | CCD |
| Collection date | 2009-05-15 |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 25.140, 54.360, 61.800 |
| Unit cell angles | 90.00, 95.45, 90.00 |
Refinement procedure
| Resolution | 40.740 - 2.400 |
| R-factor | 0.2024 |
| Rwork | 0.201 |
| R-free | 0.22890 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1rut |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.050 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | MOLREP |
| Refinement software | BUSTER (2.9.2) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.470 |
| High resolution limit [Å] | 2.400 | 2.400 |
| Rmerge | 0.120 | 0.920 |
| Number of reflections | 6395 | |
| <I/σ(I)> | 12.3 | 1.2 |
| Completeness [%] | 97.8 | 95.8 |
| Redundancy | 3.6 | 3.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4 | 25% PEG 1500 AND 100 MM SPG, BUFFER PH 4.0 |
