2XHT
Structure of HSP90 with small molecule inhibitor bound
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 100 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 53.505, 41.871, 54.202 |
| Unit cell angles | 90.00, 116.11, 90.00 |
Refinement procedure
| Resolution | 31.740 - 2.270 |
| R-factor | 0.2286 |
| Rwork | 0.225 |
| R-free | 0.29690 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| Refinement software | BUSTER-TNT (2.5.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 31.570 |
| High resolution limit [Å] | 2.300 |
| Rmerge | 0.080 |
| Number of reflections | 9778 |
| Completeness [%] | 94.0 |
| Redundancy | 2.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
