2XG7
Crystal Structure of BST2-Tetherin Ectodomain expressed in HEK293T cells
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-04-30 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 28.860, 91.860, 146.960 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 77.890 - 3.450 |
R-factor | 0.27038 |
Rwork | 0.269 |
R-free | 0.29795 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3MKX |
RMSD bond length | 0.012 |
RMSD bond angle | 1.379 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0074) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.950 | 3.640 |
High resolution limit [Å] | 3.450 | 3.450 |
Rmerge | 0.110 | 0.710 |
Number of reflections | 5576 | |
<I/σ(I)> | 8.9 | 2.5 |
Completeness [%] | 99.2 | 99.4 |
Redundancy | 6.8 | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 8% PEG8000, 0.1M TRIS-HCL PH 8.5 |