2XEU
Ring domain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-4 |
| Synchrotron site | ESRF |
| Beamline | ID14-4 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC QUANTUM 315r |
| Spacegroup name | P 41 3 2 |
| Unit cell lengths | 72.616, 72.616, 72.616 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 18.150 - 1.500 |
| R-factor | 0.16972 |
| Rwork | 0.168 |
| R-free | 0.19727 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.439 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SHELX |
| Refinement software | REFMAC (5.6.0073) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 18.000 | 1.550 |
| High resolution limit [Å] | 1.500 | 1.500 |
| Rmerge | 0.060 | 0.430 |
| Number of reflections | 10402 | |
| <I/σ(I)> | 18 | 2.9 |
| Completeness [%] | 99.8 | 100 |
| Redundancy | 9 | 7.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
