2XCY
Crystal structure of Aspergillus fumigatus sialidase
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 HF |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2010-02-23 |
| Detector | RIGAKU CCD |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 75.890, 58.190, 94.700 |
| Unit cell angles | 90.00, 100.01, 90.00 |
Refinement procedure
| Resolution | 12.400 - 1.840 |
| R-factor | 0.15528 |
| Rwork | 0.153 |
| R-free | 0.19406 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.134 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | SHELX |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 12.400 | 1.940 |
| High resolution limit [Å] | 1.840 | 1.840 |
| Rmerge | 0.060 | 0.200 |
| Number of reflections | 59980 | |
| <I/σ(I)> | 15.6 | 5.2 |
| Completeness [%] | 84.2 | 64.8 |
| Redundancy | 3.1 | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
