2WY0
Crystal structure of mouse angiotensinogen in the oxidised form with space group P6122
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-09-13 |
| Detector | ADSC CCD |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 64.650, 64.650, 461.820 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 76.920 - 2.380 |
| R-factor | 0.208 |
| Rwork | 0.206 |
| R-free | 0.25300 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.475 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALEPACK |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.5.0099) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 76.900 | 2.500 |
| High resolution limit [Å] | 2.380 | 2.380 |
| Rmerge | 0.050 | 0.400 |
| Number of reflections | 23004 | |
| <I/σ(I)> | 15.9 | 3.1 |
| Completeness [%] | 93.9 | 64.2 |
| Redundancy | 3.7 | 2.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4.25 | 1.6-2 NA2HPO4, PH4.25 |
