2WW7
foldon containing beta-turn mimic
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-02-02 |
Detector | ADSC CCD |
Spacegroup name | P 1 |
Unit cell lengths | 27.730, 28.500, 48.755 |
Unit cell angles | 77.25, 88.00, 69.45 |
Refinement procedure
Resolution | 26.020 - 1.060 |
R-factor | 0.10832 |
Rwork | 0.108 |
R-free | 0.14024 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1nay |
RMSD bond length | 0.010 |
RMSD bond angle | 2.809 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.120 |
High resolution limit [Å] | 1.060 | 1.060 |
Rmerge | 0.030 | 0.070 |
Number of reflections | 58056 | |
<I/σ(I)> | 19.2 | 9.5 |
Completeness [%] | 94.1 | 86.8 |
Redundancy | 2 | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 9 MM POTASSIUM PHOSPHATE, PH 7.0, 10% D2O |