2WW6
foldon containing D-amino acids in turn positions
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-02-02 |
Detector | ADSC CCD |
Spacegroup name | P 32 |
Unit cell lengths | 29.830, 29.830, 75.080 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 17.980 - 0.980 |
R-factor | 0.12979 |
Rwork | 0.129 |
R-free | 0.14710 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1nay |
RMSD bond length | 0.010 |
RMSD bond angle | 1.246 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.030 |
High resolution limit [Å] | 0.980 | 0.980 |
Rmerge | 0.050 | 0.280 |
Number of reflections | 42623 | |
<I/σ(I)> | 10.4 | 2.8 |
Completeness [%] | 99.2 | 98.4 |
Redundancy | 2.3 | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 9 MM POTASSIUM PHOSPHATE, PH 7.0, 10% D2O |