2WUI
Crystal Structure of MexZ, a key repressor responsible for antibiotic resistance in Pseudomonas aeruginosa.
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 287 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Wavelength(s) | 1.0000, 0.9791, 0.9793, 0.9757 |
| Spacegroup name | H 3 2 |
| Unit cell lengths | 177.055, 177.055, 54.658 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 31.384 - 2.900 |
| R-factor | 0.2291 |
| Rwork | 0.227 |
| R-free | 0.27680 |
| Structure solution method | MAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.729 |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 88.500 |
| High resolution limit [Å] | 2.900 |
| Rmerge | 0.080 |
| Number of reflections | 7354 |
| <I/σ(I)> | 6.6 |
| Completeness [%] | 99.5 |
| Redundancy | 5.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
