2WQT
Dodecahedral assembly of MhpD
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-09-01 |
Detector | ADSC CCD |
Spacegroup name | H 3 |
Unit cell lengths | 207.350, 207.350, 545.471 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 35.260 - 2.800 |
R-factor | 0.22253 |
Rwork | 0.222 |
R-free | 0.23382 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1sv6 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.313 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0088) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.400 | 2.950 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.140 | 0.530 |
Number of reflections | 210704 | |
<I/σ(I)> | 6.7 | 1.8 |
Completeness [%] | 97.9 | 95.7 |
Redundancy | 2.2 | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 3.2 | 1M NA/K PHOSPHATE PH3.2 |