2WQA
Complex of TTR and RBP4 and Oleic Acid
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL11-1 |
| Synchrotron site | SSRL |
| Beamline | BL11-1 |
| Temperature [K] | 105 |
| Detector technology | CCD |
| Collection date | 2007-10-14 |
| Detector | ADSC CCD |
| Spacegroup name | P 41 |
| Unit cell lengths | 138.662, 138.662, 122.789 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 92.060 - 2.850 |
| R-factor | 0.2279 |
| Rwork | 0.227 |
| R-free | 0.25319 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1jyd |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.562 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.990 |
| High resolution limit [Å] | 2.850 | 2.850 |
| Rmerge | 0.060 | 0.670 |
| Number of reflections | 54072 | |
| <I/σ(I)> | 21.97 | 2.95 |
| Completeness [%] | 99.5 | 99.5 |
| Redundancy | 7.5 | 7.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
