2WKK
Identification of the glycan target of the nematotoxic fungal galectin CGL2 in Caenorhabditis elegans
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-01-28 |
| Detector | RAYONIX |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 66.210, 80.620, 120.630 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 48.295 - 1.500 |
| R-factor | 0.1511 |
| Rwork | 0.150 |
| R-free | 0.18590 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1ulg |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.685 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.300 | 1.600 |
| High resolution limit [Å] | 1.500 | 1.500 |
| Rmerge | 0.070 | 0.790 |
| Number of reflections | 17766 | |
| <I/σ(I)> | 23.08 | 2.74 |
| Completeness [%] | 99.7 | 98.3 |
| Redundancy | 12.68 | 8.17 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
