2WK8

Structure of holo form of Vibrio cholerae CqsA

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	100
Spacegroup name	P 21 21 2
Unit cell lengths	177.337, 70.134, 70.625
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	27.830 - 2.100
R-factor	0.201
Rwork	0.197
R-free	0.25800
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.008
RMSD bond angle	1.211
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	28.000	2.140
High resolution limit [Å]	2.100	2.100
Rmerge	0.080	0.540
Number of reflections	50632
<I/σ(I)>	15.3	2.2
Completeness [%]	97.0	96
Redundancy	5.1	4.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1