2WGQ
Zinc substituted E Coli Copper Amine Oxidase, a model for the precursor for 2,4,5-trihydroxyphenylalaninequinone formation
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX7.2 |
| Synchrotron site | SRS |
| Beamline | PX7.2 |
| Temperature [K] | 300 |
| Detector technology | IMAGE PLATE |
| Collection date | 1997-03-01 |
| Detector | MARRESEARCH |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 134.680, 166.210, 79.420 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 39.720 - 2.500 |
| R-factor | 0.2071 |
| Rwork | 0.204 |
| R-free | 0.26398 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1spu |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.583 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC (5.5.0072) |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
