2WBV
Canine adenovirus 2 fibre head in complex with sialic acid
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-09-20 |
| Detector | ADSC QUANTUM |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 215.000, 61.250, 143.110 |
| Unit cell angles | 90.00, 131.67, 90.00 |
Refinement procedure
| Resolution | 46.130 - 1.900 |
| R-factor | 0.159 |
| Rwork | 0.157 |
| R-free | 0.19500 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2j2j |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.266 |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 46.100 | 1.970 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rmerge | 0.150 | 0.400 |
| Number of reflections | 109731 | |
| <I/σ(I)> | 10.22 | 4.06 |
| Completeness [%] | 99.4 | 98.8 |
| Redundancy | 3.7 | 3.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5% PEG 4000, 5% ISOPROPANOL, 0.1 M HEPES PH 7.4 |
