2WAL
Crystal Structure of human GADD45gamma
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.2 |
Synchrotron site | BESSY |
Beamline | 14.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-03-12 |
Detector | MARRESEARCH |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 108.717, 108.717, 73.371 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.810 - 2.400 |
R-factor | 0.216 |
Rwork | 0.215 |
R-free | 0.25100 |
Structure solution method | MAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.011 |
RMSD bond angle | 1.308 |
Data reduction software | XDS |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 20.000 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.070 | |
Number of reflections | 21647 | |
<I/σ(I)> | 18.7 | |
Completeness [%] | 93.0 | 80.3 |
Redundancy | 7.09 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 2 M MALONATE, 0.1 M BENZONATE, PH 5.5 |