2W9P
Crystal Structure of Potato Multicystatin
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.2.1 |
| Synchrotron site | ALS |
| Beamline | 8.2.1 |
| Temperature [K] | 287 |
| Detector technology | IMAGE PLATE |
| Detector | ADSC IMAGE PLATE |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 210.850, 85.710, 96.860 |
| Unit cell angles | 90.00, 100.60, 90.00 |
Refinement procedure
| Resolution | 10.000 - 2.700 |
| R-factor | 0.212 |
| Rwork | 0.212 |
| R-free | 0.24600 |
| Structure solution method | MAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.014 |
| RMSD bond angle | 3.190 |
| Refinement software | X-PLOR (NULL) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 2.700 |
| Rmerge | 0.060 |
| Number of reflections | 40548 |
| Completeness [%] | 88.4 |
| Redundancy | 5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
