2W94
Native structure of the Discoidin I from Dictyostelium discoideum at 1.8 angstrom resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-06-20 |
Detector | ADSC CCD |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 72.530, 274.371, 85.928 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.600 - 1.800 |
R-factor | 0.16679 |
Rwork | 0.165 |
R-free | 0.20593 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vm9 |
RMSD bond length | 0.017 |
RMSD bond angle | 1.496 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0066) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.600 | 1.840 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.070 | 0.230 |
Number of reflections | 29532 | |
<I/σ(I)> | 5.9 | 2 |
Completeness [%] | 94.8 | 94.8 |
Redundancy | 4 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 1.5 M LISO4 100 MM HEPES 7.5 |