2VUE
Human serum albumin complexed with 4Z,15E-bilirubin-IX-alpha
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | X11 |
| Temperature [K] | 298 |
| Detector technology | CCD |
| Collection date | 2003-02-15 |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 |
| Unit cell lengths | 55.090, 55.540, 119.830 |
| Unit cell angles | 81.22, 90.70, 65.42 |
Refinement procedure
| Resolution | 35.070 - 2.420 |
| R-factor | 0.218 |
| Rwork | 0.218 |
| R-free | 0.27300 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2bxa |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.300 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | CNS |
| Refinement software | CNS (1.2) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 35.070 | 2.570 |
| High resolution limit [Å] | 2.420 | 2.420 |
| Rmerge | 0.040 | 0.310 |
| Number of reflections | 45968 | |
| <I/σ(I)> | 9.8 | 2.2 |
| Completeness [%] | 94.9 | 85.8 |
| Redundancy | 1.9 | 1.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | SEE PAPER, pH 7 |
