2VTG

Crystal Structure of Human Iba2, trigonal crystal form

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	BESSY BEAMLINE 14.1
Synchrotron site	BESSY
Beamline	14.1
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Spacegroup name	P 32 2 1
Unit cell lengths	70.530, 70.530, 95.190
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	61.080 - 2.450
R-factor	0.205
Rwork	0.204
R-free	0.23200
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1wy9
RMSD bond length	0.016
RMSD bond angle	1.667
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	REFMAC (5.3.0040)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	2.580
High resolution limit [Å]	2.450	2.450
Rmerge	0.060	0.650
Number of reflections	10457
<I/σ(I)>	20.5	3.5
Completeness [%]	99.6	99.9
Redundancy	7.9	8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1