2VQ9
RNASE ZF-3E
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX10.1 |
Synchrotron site | SRS |
Beamline | PX10.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-07-05 |
Detector | ADSC CCD |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 43.168, 60.964, 115.229 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.340 - 1.850 |
R-factor | 0.2 |
Rwork | 0.198 |
R-free | 0.25400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vq8 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.548 |
Data reduction software | HKL (SUITE) |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.4.0066) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.920 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.120 | 0.250 |
Number of reflections | 13420 | |
<I/σ(I)> | 14.5 | 5.1 |
Completeness [%] | 98.8 | 90.6 |
Redundancy | 14 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 25% PEG 4000, 0.2M LITHIUM CHLORIDE, 0.1M TRIS-HCL PH 8.5 |