2VOE
Crystal structure of Rv2780 from M. tuberculosis H37Rv
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 |
| Temperature [K] | 298 |
| Detector technology | IMAGE PLATE |
| Detector | MARRESEARCH |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 173.891, 127.078, 135.954 |
| Unit cell angles | 90.00, 115.04, 90.00 |
Refinement procedure
| Resolution | 123.090 - 2.600 |
| R-factor | 0.19837 |
| Rwork | 0.196 |
| R-free | 0.25120 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.864 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 25.000 |
| High resolution limit [Å] | 2.600 |
| Rmerge | 0.110 |
| Number of reflections | 46867 |
| <I/σ(I)> | 9.6 |
| Completeness [%] | 97.6 |
| Redundancy | 1.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
