2VKD
CRYSTAL STRUCTURE OF THE CATALYTIC DOMAIN OF LETHAL TOXIN FROM CLOSTRIDIUM SORDELLII IN COMPLEX WITH UDP-GLC AND MANGANESE ION
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.2 |
Synchrotron site | BESSY |
Beamline | 14.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 57.287, 190.322, 204.419 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 90.170 - 2.530 |
R-factor | 0.247 |
Rwork | 0.244 |
R-free | 0.28800 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.108 |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 90.170 | 2.620 |
High resolution limit [Å] | 2.530 | 2.530 |
Rmerge | 0.120 | 0.410 |
Number of reflections | 75590 | |
<I/σ(I)> | 12.1 | 4.3 |
Completeness [%] | 99.7 | 100 |
Redundancy | 5.9 | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |