2VJ2
Human Jagged-1, domains DSL and EGFs1-3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-04-21 |
Detector | ADSC CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 61.000, 102.300, 62.700 |
Unit cell angles | 90.00, 114.30, 90.00 |
Refinement procedure
Resolution | 48.500 - 2.500 |
R-factor | 0.221 |
Rwork | 0.220 |
R-free | 0.23900 |
Structure solution method | SIRAS |
Starting model (for MR) | NONE |
RMSD bond length | 0.007 |
RMSD bond angle | 0.716 |
Data scaling software | SCALA |
Phasing software | autoSHARP |
Refinement software | TNT (5.6.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 57.100 | 2.740 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.090 | 0.420 |
Number of reflections | 11962 | |
<I/σ(I)> | 13.1 | 3.3 |
Completeness [%] | 98.6 | 98.6 |
Redundancy | 3.7 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 8.5% (W/V) PEG4000, 100MM IMIDAZOLE -MALATE, PH7.0 |