2VIU
INFLUENZA VIRUS HEMAGGLUTININ
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | LURE BEAMLINE DW32 |
| Synchrotron site | LURE |
| Beamline | DW32 |
| Detector technology | IMAGE PLATE |
| Collection date | 1997-04-08 |
| Detector | MARRESEARCH |
| Spacegroup name | P 21 3 |
| Unit cell lengths | 144.400, 144.400, 144.400 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 * - 2.500 |
| R-factor | 0.213 * |
| Rwork | 0.210 |
| R-free | 0.23900 * |
| RMSD bond length | 0.011 |
| RMSD bond angle | 25.000 * |
| Data reduction software | HKL |
| Phasing software | X-PLOR (3.84) |
| Refinement software | X-PLOR (3.84) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 2.450 |
| Rmerge | 0.055 |
| Total number of observations | 163053 * |
| Number of reflections | 36234 |
| Completeness [%] | 99.9 |
| Redundancy | 4.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 70 (mg/ml) | |
| 2 | 1 | drop | 0.15 (M) | ||
| 3 | 1 | drop | 0.05 (%) | ||
| 4 | 1 | reservoir | citrate | 1.18 (M) | |
| 5 | 1 | reservoir | 0.05 (%) |
