2VG4
Rv2361 native
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-2 |
| Synchrotron site | ESRF |
| Beamline | ID14-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Wavelength(s) | 0.933 |
| Spacegroup name | P 32 |
| Unit cell lengths | 87.300, 87.300, 183.800 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 52.000 - 2.600 |
| R-factor | 0.23 |
| Rwork | 0.216 |
| R-free | 0.25500 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 69.000 |
| High resolution limit [Å] | 2.600 |
| Rmerge | 0.140 |
| Number of reflections | 44230 |
| <I/σ(I)> | 8.4 |
| Completeness [%] | 84.0 |
| Redundancy | 2.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
