2VCB

Family 89 Glycoside Hydrolase from Clostridium perfringens in complex with PUGNAc

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	113.15
Spacegroup name	P 61
Unit cell lengths	90.704, 90.704, 252.467
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	20.000 - 2.200
R-factor	0.211
Rwork	0.208
R-free	0.25100
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.008
RMSD bond angle	1.125
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	29.690
High resolution limit [Å]	2.200
Rmerge	0.070
Number of reflections	53561
Completeness [%]	90.3
Redundancy	2.61

Crystallization Conditions

crystal ID	method	pH	temperature	details
1