2VCA

Family 89 glycoside hydrolase from Clostridium perfringens in complex with beta-N-acetyl-D-glucosamine

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	113.15
Spacegroup name	P 61
Unit cell lengths	90.773, 90.773, 252.779
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	20.000 - 2.050
R-factor	0.192
Rwork	0.190
R-free	0.23000
Structure solution method	OTHER
RMSD bond length	0.008
RMSD bond angle	1.321
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	29.710
High resolution limit [Å]	2.050
Rmerge	0.080
Number of reflections	72843
Completeness [%]	99.1
Redundancy	4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1