2VC4
Ricin A-Chain (Recombinant) E177D Mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I711 |
Synchrotron site | MAX II |
Beamline | I711 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2000-06-17 |
Detector | MARRESEARCH |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 67.400, 67.400, 140.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.490 - 1.390 |
R-factor | 0.183 |
Rwork | 0.182 |
R-free | 0.19900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ift |
RMSD bond length | 0.012 |
RMSD bond angle | 1.419 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CCP4 |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.440 |
High resolution limit [Å] | 1.390 | 1.390 |
Rmerge | 0.030 | 0.110 |
Number of reflections | 60577 | |
<I/σ(I)> | 41.6 | 6.8 |
Completeness [%] | 91.6 | 82.2 |
Redundancy | 4 | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.2 | pH 4.2 |