2V16

Crystal Structure of Renin with Inhibitor 3

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	ENRAF-NONIUS FR571
Temperature [K]	100
Detector technology	AREA DETECTOR
Collection date	1991-01-01
Detector	DELFT INSTRUMENTS
Spacegroup name	P 21 3
Unit cell lengths	142.900, 142.900, 142.900
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 2.800
R-factor	0.214
Rwork	0.214
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	MADNESS
Refinement software	TNT

Data quality characteristics

	Overall
Low resolution limit [Å]	10.000
High resolution limit [Å]	2.800
Rmerge	0.100
Number of reflections	23603
Completeness [%]	98.0
Redundancy	2.53

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		4.5		pH 4.5