2V13

Crystal Structure of Renin with Inhibitor 7

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	ENRAF-NONIUS FR571
Temperature [K]	100
Detector technology	AREA DETECTOR
Collection date	1993-01-01
Detector	DELFT
Spacegroup name	P 41 21 2
Unit cell lengths	98.400, 98.400, 95.600
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 2.800
R-factor	0.228
Rwork	0.228
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.022
RMSD bond angle	3.730
Data reduction software	MADNESS
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	10.000
High resolution limit [Å]	2.900
Rmerge	0.060
Number of reflections	10676
Completeness [%]	98.0
Redundancy	3.58

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		3		pH 3