2TLX
THERMOLYSIN (NATIVE)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX9.6 |
Synchrotron site | SRS |
Beamline | PX9.6 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 1998-07-01 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 94.145, 94.145, 131.616 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 1.650 |
Rwork | 0.163 |
R-free | 0.18800 * |
Structure solution method | ISOMORPHOUS REPLACEMENT |
Starting model (for MR) | 1lnf |
RMSD bond length | 0.016 |
RMSD bond angle | 0.800 * |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.740 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.076 | 0.352 |
Number of reflections | 41876 | |
<I/σ(I)> | 6.2 | 1.8 |
Completeness [%] | 100.0 | 100 |
Redundancy | 5 | 5.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 7.5 | pH 7.5 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | TLN | 4.6 (mM) | |
2 | 1 | 1 | DMSO | 45 (%) | |
3 | 1 | 1 | Tris-HCl | 50 (mM) | |
4 | 1 | 1 | 2.5 (M) |