2SIL

THE STRUCTURES OF SALMONELLA TYPHIMURIUM LT2 NEURAMINIDASE AND ITS COMPLEX WITH A TRANSITION STATE ANALOGUE AT 1.6 ANGSTROMS RESOLUTION

Replaces:  1SIL

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	47.500, 82.500, 91.900
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 1.600
R-factor	0.163 *
Rwork	0.166
RMSD bond length	0.014
RMSD bond angle	3.170
Phasing software	X-PLOR
Refinement software	TNT

Data quality characteristics

	Overall
High resolution limit [Å]	1.600 *
Rmerge	0.059 *
Total number of observations	59728 *
Number of reflections	35140 *
Completeness [%]	69.6 *
Redundancy	1.7 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	neuraminidase	10-15 (mg/ml)
2	1	drop	potassium phosphate	1.9 (M)
3	1	reservoir	potassium phosphate	2.1 (M)