2RGW
Catalytic Subunit of M. jannaschii Aspartate Transcarbamoylase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 295 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 139.900, 91.890, 154.200 |
Unit cell angles | 90.00, 98.30, 90.00 |
Refinement procedure
Resolution | 100.000 - 2.800 |
Rwork | 0.199 |
R-free | 0.25700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3csu |
RMSD bond length | 0.010 |
RMSD bond angle | 1.200 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | EPMR |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 100.000 |
High resolution limit [Å] | 2.800 |
Number of reflections | 37976 |
<I/σ(I)> | 12.1 |
Redundancy | 1.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | ammonium sulfate, isopropanol, VAPOR DIFFUSION, SITTING DROP, temperature 295K |