2RDL
Hamster Chymase 2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Detector technology | CCD |
| Collection date | 2006-07-21 |
| Detector | ADSC QUANTUM 210 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 71.272, 71.272, 198.575 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 35.000 - 2.500 |
| Rwork | 0.186 |
| R-free | 0.25300 |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.708 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 35.000 |
| High resolution limit [Å] | 2.500 |
| Number of reflections | 18529 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 298 | 25% PEG 3350, 0.1 M Tris-HCl, pH 8.5, and 0.2 M Ammonium Sulfate, VAPOR DIFFUSION, SITTING DROP, temperature 298K |
