2RC6
Refined structure of FNR from Leptospira interrogans bound to NADP+
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU ULTRAX 18 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2005-01-01 |
Detector | MAR scanner 345 mm plate |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 67.168, 112.251, 92.399 |
Unit cell angles | 90.00, 93.19, 90.00 |
Refinement procedure
Resolution | 33.532 - 2.700 |
R-factor | 0.2367 |
Rwork | 0.235 |
R-free | 0.27590 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.771 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 92.450 | 112.510 | 2.750 |
High resolution limit [Å] | 2.610 | 8.250 | 2.610 |
Rmerge | 0.110 | 0.045 | 0.734 |
Number of reflections | 36768 | ||
<I/σ(I)> | 6.3 | 11.6 | 1 |
Completeness [%] | 87.8 | 99.9 | 67.4 |
Redundancy | 3 | 3.8 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 291 | 27% PEG3350, 0.3M ammonium fluoride, 50mM Tris-HCL buffer, pH 7.0, vapor diffusion, temperature 291K |